Hydrazine → HCID 21947598, Verbindung
Reaktionsgleichung
[CH3:1][C:2]1[N:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11][N:12]2C(=O)C3C(=CC=CC=3)C2=O)=[CH:4][CH:3]=1.NN>C(O)C>[CH3:1][C:2]1[N:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11][NH2:12])=[CH:4][CH:3]=1Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
A mixture of 2-4 (7.2 g, 24.5 mmol), hydrazine (3.8 mL), and ethanol (500 mL) was heated at reflux for 4 hours. The resulting mixture was cooled and filtered, and the filtrate concentrated to give 2-5 as a yellow solid (4.7 g) contaminated with some phthalhydrazide.
Aufarbeitung
- temperaturewas heated
- temperatureat reflux for 4 hours
- temperatureThe resulting mixture was cooled
- filtrationfiltered
- concentrationthe filtrate concentrated
Quellen und Nachweise
- ORD-Eintrag
- ord-0f76b292b1834ee9a3cb1ea97addaf33
- Quelldatensatz
- uspto-grants-2006_09
- Patentnummer
- US07109191B2
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