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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 22150Erstellt: 23. Oktober 2026

1-Dodecanol → Lactic acid hydroxycaproic acid

https://huagongshe.com/de/reaction/22150

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1-DodecanolHCID 8193—
Edukt2-ethylhexanoic acid tin(II) saltHCID 9318—
Eduktepsilon-CAPROLACTONEHCID 10401—
EduktLactide, L-HCID 107983—
LösungsmittelTolueneHCID 1140—
ProduktLactic acid hydroxycaproic acidHCID 86747420—

Reaktionsschritte

The same procedure as in Preparation Example 3 was effected except that 1441 g (10 mols) of L-lactide, 1140 g (10 mols) of ε-caprolactone and 10 ml of a toluene solution containing 0.26 g of stannous octoate, and 5 g of lauryl alcohol were used and that reaction was carried out at 160° C. for 10 hours, thereby obtaining a lactic acid-hydroxycaproic acid copolymer (hereinafter referred to as "PCLA1").

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUSRE034984
Quelldatensatzuspto-grants-1995_06
ORD IDord-d9402f9cd14742bf8acde96329546880
Quellennotizuspto-grants-1995_06