Hydrochloric Acid → HCID 57422604, Verbindung

Reaktionsgleichung

[CH:1]1([C:6]([CH:8]([NH:13]C(=O)OC(C)(C)C)[CH:9]([CH3:12])[CH2:10][CH3:11])=[O:7])[CH2:5][CH2:4][CH2:3][CH2:2]1.[ClH:21]>>[Cl-:21].[CH:1]1([C:6](=[O:7])[CH:8]([NH3+:13])[CH:9]([CH3:12])[CH2:10][CH3:11])[CH2:5][CH2:4][CH2:3][CH2:2]1

Komponenten

Edukt 2

HCID 313Hydrochloric Acid

HCID 21952981HCID 21952981, Verbindung

Produkt 1

HCID 57422604HCID 57422604, Verbindung

Versuchsvorschrift

4 (0.18 g, 0.63 mmol) was dissolved in 2 ml HCl (7 N in dioxane). After completion of the reaction the solvent was removed and the resulting oil was purified by column chromatography on silical gel using a chloroform/methanol/water gradient. The resulting oil was triturated with ether.

Aufarbeitung

customAfter completion of the reaction the solvent
customwas removed
customthe resulting oil was purified by column chromatography on silical gel
customThe resulting oil was triturated with ether

Quellen und Nachweise

ORD-Eintrag: ord-a73c945cf85441cbbaeb2ba84ab204bc
Quelldatensatz: uspto-grants-2006_09
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07109347B2

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