HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Epibromohydrin → Tert-butyldimethyl(4-(oxiran-2-ylmethoxy)phenoxy)silane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Epibromohydrin | HCID 18430 | — |
| Edukt | 4-(tert-Butyldimethylsiloxy)phenol | HCID 597388 | — |
| Produkt | Tert-butyldimethyl(4-(oxiran-2-ylmethoxy)phenoxy)silane | HCID 19385012 | 21% |
Reaktionsschritte
Synthesis followed SP3a, using 4.1 mmol 4-(tert-Butyl-dimethyl-silanyloxy)-phenol and racemic epibromohydrine to give the title compound upon purification by Flash Master Personal (20 g silica gel cartridge, PE to PE/ethyl acetate 15:1) with 21% yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08207174B2 |
| Quelldatensatz | uspto-grants-2012_06 |
| ORD ID | ord-95e5a9dc1d794b0b99703425051ff954 |
| Quellennotiz | uspto-grants-2012_06 |