HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Methylpiperazine → 5-Amino-2-(4-methylpiperazin-1-yl)benzonitrile
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Methylpiperazine | HCID 53167 | — |
| Edukt | 2-Chloro-5-nitrobenzonitrile | HCID 85504 | — |
| Produkt | 5-Amino-2-(4-methylpiperazin-1-yl)benzonitrile | HCID 17609581 | 62,5% |
Reaktionsschritte
By the reaction and treatment in the same manner as in Starting Material Synthetic Example 4 using 2-chloro-5-nitrobenzonitrile (15 g) and methylpiperazine (9.8 g), the title compound (11.1 g) was obtained. melting point: 45-46° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07112594B2 |
| Quelldatensatz | uspto-grants-2006_09 |
| ORD ID | ord-58fcb8b3c4f747289de79d546576b89c |
| Quellennotiz | uspto-grants-2006_09 |