Ammonium Chloride → HCID 178425624, Verbindung
Reaktionsgleichung
[CH3:1][C:2]1([CH3:10])[CH2:7][CH2:6][C:5](OC)=[N:4][CH2:3]1.[Cl-:11].[NH4+:12]>C(O)C>[ClH:11].[CH3:1][C:2]1([CH3:10])[CH2:3][NH:4][C:5](=[NH:12])[CH2:6][CH2:7]1Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
The mixture of 3,3-dimethyl-6-methoxy-2,3,4,5-tetrahydropyridine (9.0 g, 64 mmol) and ammonium chloride (3.4 g, 64 mmol) in dry ethanol (160 mL) was heated to reflux for 2 h. The reaction mixture was then concentrated under reduced pressure and the titled compound was obtained as a white solid (9.9 g, 94.6%).
Aufarbeitung
- temperaturewas heated
- temperatureto reflux for 2 h
- concentrationThe reaction mixture was then concentrated under reduced pressure
Quellen und Nachweise
- ORD-Eintrag
- ord-32014185ff6946bea573072723556ba0
- Quelldatensatz
- uspto-grants-2006_09
- Patentnummer
- US07112582B2
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