Trifluoroacetic acid → HCID 178484433, Verbindung
Reaktionsgleichung
[Br:1][C:2]1[CH:3]=[C:4]2[N:10]=[C:9]([C:11]3[CH:16]=[CH:15][C:14]([OH:17])=[CH:13][CH:12]=3)[NH:8][C:5]2=[N:6][CH:7]=1.Br[CH2:19][CH2:20][N:21](C)[C:22](=O)OC(C)(C)C.FC(F)(F)C(O)=O>>[Br:1][C:2]1[CH:3]=[C:4]2[N:10]=[C:9]([C:11]3[CH:12]=[CH:13][C:14]([O:17][CH2:19][CH2:20][NH:21][CH3:22])=[CH:15][CH:16]=3)[NH:8][C:5]2=[N:6][CH:7]=1Komponenten
4
Versuchsvorschrift
The title compound was prepared from 4-(6-bromo-3H-imidazo[4,5-b]pyridin-2-yl)phenol and tert-butyl 2-bromoethyl(methyl)carbamate using the method described in Example 41, followed by deprotection using trifluoroacetic acid.
Quellen und Nachweise
- ORD-Eintrag
- ord-1b416a1ebfbf40a8933c48cffe35cef2
- Quelldatensatz
- uspto-grants-2008_08