5-Bromopyrimidine → HCID 11659866, Verbindung
Reaktionsgleichung
[CH3:1][C:2]1[N:3]=[C:4]([NH:7][C:8]([C:10]2[C:15]([NH2:16])=[CH:14][CH:13]=[C:12]([CH3:17])[N:11]=2)=[O:9])[S:5][CH:6]=1.Br[C:19]1[CH:20]=[N:21][CH:22]=[N:23][CH:24]=1>>[CH3:1][C:2]1[N:3]=[C:4]([NH:7][C:8]([C:10]2[C:15]([NH:16][C:19]3[CH:20]=[N:21][CH:22]=[N:23][CH:24]=3)=[CH:14][CH:13]=[C:12]([CH3:17])[N:11]=2)=[O:9])[S:5][CH:6]=1Komponenten
3
Versuchsvorschrift
The title compound, light brown solid, MS (ISP): m/e=327.0 (M+H+), was prepared from 3-Amino-6-methyl-pyridine-2-carboxylic acid (4-methyl-thiazol-2-yl)-amide in accordance with the general method of example 20 using 5-bromopyrimidine instead of 3-bromo-pyridine.
Quellen und Nachweise
- ORD-Eintrag
- ord-77a7e724bf464b0c90b668664efe88c7
- Quelldatensatz
- uspto-grants-2008_08
- Patentnummer
- US07414060B2
Notizen zur Reaktion
Wird geladen…