5-Bromopyrimidine → HCID 11659570, Verbindung
Reaktionsgleichung
[CH3:1][N:2]1[CH:6]=[CH:5][C:4]([NH:7][C:8]([C:10]2[C:15]([NH2:16])=[CH:14][CH:13]=[C:12]([CH3:17])[N:11]=2)=[O:9])=[N:3]1.Br[C:19]1[CH:20]=[N:21][CH:22]=[N:23][CH:24]=1>>[CH3:1][N:2]1[CH:6]=[CH:5][C:4]([NH:7][C:8]([C:10]2[C:15]([NH:16][C:19]3[CH:20]=[N:21][CH:22]=[N:23][CH:24]=3)=[CH:14][CH:13]=[C:12]([CH3:17])[N:11]=2)=[O:9])=[N:3]1Komponenten
3
Versuchsvorschrift
The title compound, light brown solid, MS (ISP): m/e=310.4 (M+H+), was prepared from 3-Amino-6-methyl-pyridine-2-carboxylic acid (1-methyl-1H-pyrazol-3-yl)-amide in accordance with the general method of example 20 using 5-bromopyrimidine instead of 3-bromo-pyridine.
Quellen und Nachweise
- ORD-Eintrag
- ord-c8b212fb8fc340109f0cbf23bc621371
- Quelldatensatz
- uspto-grants-2008_08
- Patentnummer
- US07414060B2
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