Diethylamine → (2-Bromo-benzyl)-diethyl-amine
Reaktionsgleichung
[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8]Br.[CH2:10]([NH:12][CH2:13][CH3:14])[CH3:11]>C1(C)C=CC=CC=1>[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][N:12]([CH2:13][CH3:14])[CH2:10][CH3:11]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
To 1-Bromo-2-bromomethyl-benzene (2.17 g, 0.008 mmol) in toluene (15 mL) was added diethylamine (3.05 mL) and the mixture was stirred at room temperature for 14 hours. The reaction mixture was filtered and concentrated to give Example 229A as an oil.
Aufarbeitung
- filtrationThe reaction mixture was filtered
- concentrationconcentrated
Quellen und Nachweise
- ORD-Eintrag
- ord-ca758fde160a49c097dfedcef981117c
- Quelldatensatz
- uspto-grants-2008_08
- Patentnummer
- US07417040B2
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