[3-(Benzo[b]thiophen-4-yloxy)-5-methyl-hexyl]-benzyl-methyl-amine → [3-(Benzo[b]thiophen-4-yloxy)-4-methyl-pentyl]-benzyl-methyl-amine

HRID 2220353

Reaktionsgleichung

Reaktionsgleichung von HRID 2220353
[S:1]1[CH:5]=[CH:4][C:3]2[C:6]([O:10][CH:11]([CH2:23][CH:24](C)C)[CH2:12][CH2:13][N:14]([CH2:16][C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)[CH3:15])=[CH:7][CH:8]=[CH:9][C:2]1=2.[CH2:27](N(C)CCC(O)C(C)C)C1C=CC=CC=1>>[S:1]1[CH:5]=[CH:4][C:3]2[C:6]([O:10][CH:11]([CH:23]([CH3:24])[CH3:27])[CH2:12][CH2:13][N:14]([CH2:16][C:17]3[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=3)[CH3:15])=[CH:7][CH:8]=[CH:9][C:2]1=2

Komponenten

3

Edukt 2

HCID 10316919[3-(Benzo[b]thiophen-4-yloxy)-5-methyl-hexyl]-benzyl-methyl-amineHCID 179819391-(Benzyl-methyl-amino)-4-methyl-pentan-3-ol

Produkt 1

HCID 58591171[3-(Benzo[b]thiophen-4-yloxy)-4-methyl-pentyl]-benzyl-methyl-amine

Versuchsvorschrift

Using a method similar to that for [3-(Benzo[b]thiophen-4-yloxy)-5-methyl-hexyl]-benzyl-methyl-amine, 1-(benzyl-methyl-amino)-4-methyl-pentan-3-ol affords the title compound: mass spectrum (ion spray) m/z=354.3(M+1); 1H NMR (CDCl3) δ 7.49 (d, 1H), 7.43 (d, 1H), 7.31-7.19 (m, 7H), 6.85 (d, 1H), 4.48-4.44 (m, 1H), 3.51-3.43 (m, 2H), 2.61-2.48 (m, 2), 2.19 (s, 3H), 2.11-1.85 (m, 3H), 1.03 (d, 3H), 0.99 (d, 3H).

Quellen und Nachweise

ORD-Eintrag
ord-1571e7465d92422c9c55967908ec861f
Quelldatensatz
uspto-grants-2008_08
Patentnummer
US07417064B2

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