3,4-Dimethoxybenzeneacetonitrile → HCID 10405853, Verbindung
Reaktionsgleichung
[CH2:1]([O:3][C:4]1[CH:11]=[CH:10][C:7]([CH:8]=O)=[CH:6][C:5]=1[N+:12]([O-:14])=[O:13])[CH3:2].[CH3:15][O:16][C:17]1[CH:18]=[C:19]([CH:23]=[CH:24][C:25]=1[O:26][CH3:27])[CH2:20][C:21]#[N:22]>>[CH3:15][O:16][C:17]1[CH:18]=[C:19](/[C:20](=[CH:8]/[C:7]2[CH:10]=[CH:11][C:4]([O:3][CH2:1][CH3:2])=[C:5]([N+:12]([O-:14])=[O:13])[CH:6]=2)/[C:21]#[N:22])[CH:23]=[CH:24][C:25]=1[O:26][CH3:27]Komponenten
3
Versuchsvorschrift
4-Ethoxy-3-nitrobenzaldehyde (586 mg) and 3,4-dimethoxybenzyl cyanide (532 mg) were subjected to condensation in accordance with process B of (production process 2), to thereby produce the target product (425 mg, yield: 40%).
Quellen und Nachweise
- ORD-Eintrag
- ord-3e071da0e39549c5827f29421e788d7f
- Quelldatensatz
- uspto-grants-2008_05