HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 222533Erstellt: 25. Oktober 2026
2-Ethoxy-2-oxoethyl 2-butyl-4-chloro-1-{[2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate → HCID 178441701, Verbindung
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Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
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| Edukt | 2-Ethoxy-2-oxoethyl 2-butyl-4-chloro-1-{[2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate | HCID 67979259 | — |
| Lösungsmittel | Hydrochloric Acid | HCID 313 | — |
| Produkt | HCID 178441701 | HCID 178441701 | — |
Reaktionsschritte
2-Ethoxy-2-oxoethyl 2-butyl-4-chloro-1-{[2′-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate (1130 mg, 1.48 mmol) was dissolved in concentrated hydrochloric acid (24 mL). The solution was stirred at 100° C. for 30 minutes. The solution was washed with diethyl ether (2×) and the aqueous layer was concentrated in vacuo. The residue was used crude in the following step. LC-MS: m/z 495.0 (M+H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US08207208B2 |
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| Quelldatensatz | uspto-grants-2012_06 |
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| ORD ID | ord-018cd20f0477416fa71c6811ece574cb |
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| Quellennotiz | uspto-grants-2012_06 |
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