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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 222533Erstellt: 25. Oktober 2026

2-Ethoxy-2-oxoethyl 2-butyl-4-chloro-1-{[2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate → HCID 178441701, Verbindung

https://huagongshe.com/reaction/222533

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-Ethoxy-2-oxoethyl 2-butyl-4-chloro-1-{[2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylateHCID 67979259—
LösungsmittelHydrochloric AcidHCID 313—
ProduktHCID 178441701HCID 178441701—

Reaktionsbedingungen

Temperatur100 °C

Reaktionsschritte

2-Ethoxy-2-oxoethyl 2-butyl-4-chloro-1-{[2′-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate (1130 mg, 1.48 mmol) was dissolved in concentrated hydrochloric acid (24 mL). The solution was stirred at 100° C. for 30 minutes. The solution was washed with diethyl ether (2×) and the aqueous layer was concentrated in vacuo. The residue was used crude in the following step. LC-MS: m/z 495.0 (M+H).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08207208B2
Quelldatensatzuspto-grants-2012_06
ORD IDord-018cd20f0477416fa71c6811ece574cb
Quellennotizuspto-grants-2012_06