HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Formic Acid → 3-(3,4-Dimethoxyphenyl)propionic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Formic Acid | HCID 284 | — |
| Edukt | 5-(3,4-Dimethoxybenzylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione | HCID 370314 | — |
| Lösungsmittel | Triethylamine | HCID 8471 | — |
| Produkt | 3-(3,4-Dimethoxyphenyl)propionic acid | HCID 75019 | — |
Reaktionsschritte
After weighing 14.6 g (0.05 mol) of 5-(3,4-dimethoxyphenylmethylene)-2,2-dimethyl-1,3-dioxane-4,6-dione (m.p.: 173° C.) to 50 ml of the mixture of formic acid and triethylamine prepared according to Example 1, the procedure described in Example 1 was followed.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05350872 |
| Quelldatensatz | uspto-grants-1994_09 |
| ORD ID | ord-1d4a6e09e4f740589cf4bec7be7308c7 |
| Quellennotiz | uspto-grants-1994_09 |