2,2,2-Trichloroethanimidamide → HCID 178516502, Verbindung

HRID 223131

Reaktionsgleichung

Reaktionsgleichung von HRID 223131
[Cl:1][C:2]([Cl:7])([Cl:6])[C:3]([NH2:5])=[NH:4].[C:8]([O-])(=O)[CH2:9][C:10](C)=[O:11]>>[OH:11][C:10]1[CH:9]=[CH:8][N:5]=[C:3]([C:2]([Cl:7])([Cl:6])[Cl:1])[N:4]=1

Komponenten

3

Edukt 2

HCID 356082,2,2-TrichloroethanimidamideHCID 6971017Acetoacetate

Produkt 1

HCID 178516502HCID 178516502, Verbindung

Versuchsvorschrift

The carboxylic ester compounds of the present invention may be prepared by reacting trichloroacetamidine with a selected acetoacetate to form the corresponding 4-hydroxy-2-trichloromethylpyrimidine, which is then reacted with a selected carboxylic acid chloride. These general reactions are illustrated below in equations (A) and (B). In equation (A), trichloroacetamidine is reacted with ethyl 2-chloroacetoacetate to form 5-chloro-4-hydroxy-6-methyl-2-trichloromethyl-pyrimidine. In equation (B), the 5-chloro-4-hydroxy-6-methyl-2-trichloromethylpyrimidine is reacted with trichloroacetyl chloride to form 5-chloro-6-methyl-4-trichloroacetoxy-2-trichloromethylpyrimidine. ##STR3##

Quellen und Nachweise

ORD-Eintrag
ord-f5ee539350084581ab50b6a0008f2c84
Quelldatensatz
uspto-grants-1982_10
Patentnummer
US04352806

Verknüpfte Notizen

Wird geladen…