2-Bromopropane → 1-Isopropyl-4-(4-Methyl-3-nitro-phenyl)-piperazine
Reaktionsgleichung
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:13][CH2:12][NH:11][CH2:10][CH2:9]2)=[CH:4][C:3]=1[N+:14]([O-:16])=[O:15].[CH:17](Br)([CH3:19])[CH3:18]>>[CH:17]([N:11]1[CH2:10][CH2:9][N:8]([C:5]2[CH:6]=[CH:7][C:2]([CH3:1])=[C:3]([N+:14]([O-:16])=[O:15])[CH:4]=2)[CH2:13][CH2:12]1)([CH3:19])[CH3:18]Komponenten
3
Versuchsvorschrift
Beginning with 1-(4-methyl-3-nitro-phenyl)-piperazine and 1-isopropylbromide, the title compound was recovered by the procedure described in Example 2. MS m/z (rel. intensity, 70 eV) 263 (M+, 31), 249 (15), 248 (bp), 84 (15), 56 (42).
Aufarbeitung
- customthe title compound was recovered by the procedure
Quellen und Nachweise
- ORD-Eintrag
- ord-cc6a34b8cfca4a65a1a5b03d39d570c7
- Quelldatensatz
- uspto-grants-2010_05
- Patentnummer
- USRE041315E1
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