Cyclopentanone → Methyl2-[(cyclopentylamino)methyl]-2-ethyl-butanoate
Reaktionsgleichung
[CH3:1][O:2][C:3](=[O:14])[C:4]([CH2:12][CH3:13])([CH2:7][NH:8][CH:9]([CH3:11])[CH3:10])[CH2:5][CH3:6].[C:15]1(=O)CCC[CH2:16]1>>[CH3:1][O:2][C:3](=[O:14])[C:4]([CH2:7][NH:8][CH:9]1[CH2:10][CH2:16][CH2:15][CH2:11]1)([CH2:12][CH3:13])[CH2:5][CH3:6]Komponenten
3
Versuchsvorschrift
The title compound was prepared by an analogous method to the preparation of Intermediate 200, on a 50 mmol scale utilising Cyclopentanone (Aldrich; 6.33 g, 75 mmol), and distillation at 50° C. and 0.53 mbar pressure, as a clear oil (7.5 g, 65%)
Quellen und Nachweise
- ORD-Eintrag
- ord-8e6f5bfec7c5450e8aa0a3bf0972a4fd
- Quelldatensatz
- uspto-grants-2010_05
- Patentnummer
- US07709471B2
Notizen zur Reaktion
Wird geladen…