m-Anisoyl chloride → N-(6-tert.-Butyloxycarbonyl-3-cyano-4,5,6,7-tetrahvdro-thieno[2,3-c]pyridin-2-yl)-3-methoxybenzamide
Reaktionsgleichung
[CH3:1][C:2]([O:5][C:6]([N:8]1[CH2:13][CH2:12][C:11]2[C:14]([C:18]#[N:19])=[C:15]([NH2:17])[S:16][C:10]=2[CH2:9]1)=[O:7])([CH3:4])[CH3:3].[CH3:20][O:21][C:22]1[CH:23]=[C:24]([CH:28]=[CH:29][CH:30]=1)[C:25](Cl)=[O:26]>>[C:2]([O:5][C:6]([N:8]1[CH2:13][CH2:12][C:11]2[C:14]([C:18]#[N:19])=[C:15]([NH:17][C:25](=[O:26])[C:24]3[CH:28]=[CH:29][CH:30]=[C:22]([O:21][CH3:20])[CH:23]=3)[S:16][C:10]=2[CH2:9]1)=[O:7])([CH3:1])([CH3:3])[CH3:4]Komponenten
3
Versuchsvorschrift
Prepared according to general procedure A starting from 2-amino-3-cyano-4,7-dihydro-thieno[2,3-c]pyridine-6(5H)-carboxylic acid 1,1-dimethylethyl ester (compound A2) and 3-methoxybenzoyl chloride.
Aufarbeitung
- customPrepared