1-Butyl-4-chloromethyl-2-methoxy-benzene → 4-Azidomethyl-1-butyl-2-methoxy-benzene
Reaktionsgleichung
[N:1]([CH2:4][C:5]1[CH:10]=[CH:9][C:8]([C:11]2C=C[CH:14]=[CH:13][CH:12]=2)=[C:7]([O:17][CH3:18])[CH:6]=1)=[N+:2]=[N-:3].C(C1C=CC(CCl)=CC=1OC)CCC>>[N:1]([CH2:4][C:5]1[CH:10]=[CH:9][C:8]([CH2:11][CH2:12][CH2:13][CH3:14])=[C:7]([O:17][CH3:18])[CH:6]=1)=[N+:2]=[N-:3]Komponenten
3
Versuchsvorschrift
Following the same procedure for the preparation of 4-Azidomethyl-2-methoxy-biphenyl, the title compound is prepared from 1-Butyl-4-chloromethyl-2-methoxy-benzene (crude material from the previous step) in 36% yield (overall yield for 4 steps).
Aufarbeitung
- customin 36% yield (overall yield for 4 steps)
Quellen und Nachweise
- ORD-Eintrag
- ord-305d1ae7fdbf442182c910cbf7f01e89
- Quelldatensatz
- uspto-grants-2010_05
- Patentnummer
- US07713994B2
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