HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cyclohexanone → N-cyclohexylidene(3-phenoxybenzylamine)
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cyclohexanone | HCID 7967 | — |
| Edukt | 3-Phenoxy-benzylamine | HCID 1094836 | — |
| Produkt | N-cyclohexylidene(3-phenoxybenzylamine) | HCID 23332475 | 58,8% |
Reaktionsschritte
The procedure is carried out as described in Example 1(b) but with the use of 50 g (0.25 mol) of 3-phenoxybenzylamine and 25 g (0.255 mol) of cyclohexanone. Distillation leaves 41 g (0.147 mol) of N-cyclohexylidene(3-phenoxybenzylamine), corresponding to a yield of 58.7% of theory; b.p. 135°-136° C./4 Pa.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04231962 |
| Quelldatensatz | uspto-grants-1980_11 |
| ORD ID | ord-8c9b2432a9be468692207c8de8a277d2 |
| Quellennotiz | uspto-grants-1980_11 |