Trimethylsilylacetylene → 1-(3-Nitro-phenyl)-4-trimethylsilanyl-1H-[1,2,3]triazole

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

Azido-3-nitro-benzene (CAS:1516-59-2, 11.8 g, 72 mmol) were dissolved in 20 ml THF and 30 ml trimethylsilylacetylene. The reaction mixture was stirred at 60° C. for 3 days. The solvents were evaporated off and the title compound was obtained as a brown solid (16.9 g, 90%), mp 75-78° C.

Herkunft & Nachweise