Benzene → 2,3-Dimethyl-5-allyl-6-tetradecanoylhydroquinone

HRID 224469Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 224469
C([O:4][C:5]1[C:10]([C:11](=[O:25])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])=[CH:9][C:8]([OH:26])=[C:7]([CH3:27])[C:6]=1[CH3:28])C=C.[CH:29]1[CH:34]=CC=C[CH:30]=1>>[CH3:28][C:6]1[C:7]([CH3:27])=[C:8]([OH:26])[C:9]([CH2:34][CH:29]=[CH2:30])=[C:10]([C:11](=[O:25])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])[C:5]=1[OH:4]

Komponenten

3

Edukt 2

HCID 241BenzeneHCID 233332484-Hydroxy-2,3-dimethyl-6-tetradecanoylphenyl allyl ether

Produkt 1

HCID 205104582,3-Dimethyl-5-allyl-6-tetradecanoylhydroquinone

Versuchsvorschrift

90 g of the allyl ether of step 2 were heated to 210° C. under nitrogen atmosphere within 2 h. After cooling the melt was dissolved in 300 ml of benzine (boiling range: 50°-75° C.) and placed in a cool place. The precipitate formed was filtered with suction the next day.

Aufarbeitung

  1. temperatureAfter cooling the melt
  2. customThe precipitate formed
  3. filtrationwas filtered with suction the next day

Quellen und Nachweise

ORD-Eintrag
ord-7c05fbbb7b284f8d945e48ff232f998e
Quelldatensatz
uspto-grants-1980_11
Patentnummer
US04232107

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