HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2246233Erstellt: 26. Oktober 2026
Hydroxylamine → 2-Chloro-N'-hydroxy-4-[(methylsulfonyl)amino]benzenecarboximidamide
https://huagongshe.com/reaction/2246233
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Hydroxylamine | HCID 787 | — |
| Edukt | N-(3-chloro-4-cyanophenyl)methanesulfonamide | HCID 669685 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 2-Chloro-N'-hydroxy-4-[(methylsulfonyl)amino]benzenecarboximidamide | HCID 72533799 | — |
Reaktionsschritte
To a stirred solution of the product from Step A (0.13 g, 0.565 mmol) in ethanol (3 mL) was added hydroxylamine (50% in water, 1.0 mL). The reaction was heated at 90° C. for 2 h. The reaction was then concentrated to give the desired product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US07687492B2 |
|---|
| Quelldatensatz | uspto-grants-2010_03 |
|---|
| ORD ID | ord-29c660b8b31b4cfb89eb3c7c518f418c |
|---|
| Quellennotiz | uspto-grants-2010_03 |
|---|