Azobisisobutyronitrile → Acrylamido methyl-4-hydroxy benzophenone stearyl methacrylate

HRID 224683

Reaktionsgleichung

Reaktionsgleichung von HRID 224683
[Pb].[N].[C:3]([NH:7][CH2:8][C:9]1[CH:22]=[C:21]([OH:23])[CH:20]=[CH:19][C:10]=1[C:11]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)=[O:12])(=[O:6])[CH:4]=[CH2:5].[C:24]([O:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH3:47])(=[O:28])[C:25]([CH3:27])=[CH2:26].N(C(C)(C)C#N)=NC(C)(C)C#N>CC(C)=O>[C:3]([NH:7][CH2:8][C:9]1[CH:22]=[C:21]([OH:23])[CH:20]=[CH:19][C:10]=1[C:11]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)=[O:12])(=[O:6])[CH:4]=[CH2:5].[C:24]([O:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH3:47])(=[O:28])[C:25]([CH3:27])=[CH2:26]

Komponenten

6

Edukt 4

HCID 6547AzobisisobutyronitrileHCID 122600Stearyl methacrylateHCID 54571820Acrylamido methyl 4-hydroxy benzophenoneHCID 178514658HCID 178514658, Verbindung

Produkt 1

HCID 86733966Acrylamido methyl-4-hydroxy benzophenone stearyl methacrylate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 180AcetoneLösungsmittel

Reaktionsbedingungen

Temperatur
80 °C

Versuchsvorschrift

Into a 50 ml flask provided with a condenser, a nitrogen lead in tube and an agitator, there are intorduced 1 g of acrylamido methyl 4-hydroxy benzophenone, 1.5 g of stearyl methacrylate and 0.25 g of azobis-isobutyronitrile in solution in 5 ml of acetone. The resulting mixture is heated for 8 hours at 80° C.

Aufarbeitung

  1. customInto a 50 ml flask provided with a condenser

Quellen und Nachweise

ORD-Eintrag
ord-f12a8b52012e49d5a2ccfc21ae104854
Quelldatensatz
uspto-grants-1980_11
Patentnummer
US04233430

Verknüpfte Notizen

Wird geladen…