HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-tert-Butylbenzaldehyde → 4-tert-Butyltoluene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-tert-Butylbenzaldehyde | HCID 70324 | — |
| Edukt | Benzenemethanol, 4-(1,1-dimethylethyl)-, 1-acetate | HCID 105421 | — |
| Produkt | 4-tert-Butyltoluene | HCID 7390 | 83,3% |
Reaktionsschritte
If the material discharged from the electrolysis is worked up similarly to Example 1, 284.8 g of p-tert.-butylbenzaldehyde and 295.3 g of p-tert.-butylbenzyl acetate are obtained in addition to 25.2 g of unconverted p-tert.-butyltoluene. This corresponds to a yield of 83.3% and a current efficiency of 58.2%. The p-tert.-butylbenzaldehyde is separated from the p-tert.-butylbenzyl acetate by the method described in Example 1.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04235683 |
| Quelldatensatz | uspto-grants-1980_11 |
| ORD ID | ord-5cac8f11e5494aa1bdf787d75a261d71 |
| Quellennotiz | uspto-grants-1980_11 |