HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium periodate → Cis-1,4-Dimethoxy-9,10-dihydro-9,10-anthracenedicarboxaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium periodate | HCID 516896 | — |
| Edukt | 1,4-Dimethoxy-9,10-dihydro-9,10-ethanoanthracene-11,12-diol | HCID 23329608 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | Cis-1,4-Dimethoxy-9,10-dihydro-9,10-anthracenedicarboxaldehyde | HCID 88785356 | — |
Reaktionsschritte
One gram of 1,4-dimethoxy-9,10-dihydro-9,10-ethanoanthracene-11,12-diol, is suspended in 30 ml. of an aqueous solution containing 0.77 g. of potassium periodate and one ml. of ethanol. After stirring at room temperature for 24 hours the insoluble material is removed by filtration, washed well with water and dried leaving a yellow product, m.p. 129°-132° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04235996 |
| Quelldatensatz | uspto-grants-1980_11 |
| ORD ID | ord-cb2cb3b108aa4d2da3ce5f436af99830 |
| Quellennotiz | uspto-grants-1980_11 |