HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Chlorophthalic acid → 4-Chlorophthalic anhydride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Chlorophthalic acid | HCID 6964 | — |
| Edukt | 4-Chloro-1,2-dicyanobenzene | HCID 87213 | — |
| Edukt | 4-Chlorobenzene-1,2-dicarbonyl dichloride | HCID 15044562 | — |
| Produkt | 4-Chlorophthalic anhydride | HCID 67044 | — |
Reaktionsschritte
In a conventional acidic hydrolysis, the 4-chlorophthaloyl chloride or 4-chlorophthalonitrile of Examples 7 or 8 is hydrolyzed to 4-chlorophthalic acid which, upon dehydration at over 180°-200° C., will afford a high yield of 4-chlorophthalic anhydride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05233054 |
| Quelldatensatz | uspto-grants-1993_08 |
| ORD ID | ord-2124179a0f7d4cd3a9adfbf727a95a6f |
| Quellennotiz | uspto-grants-1993_08 |