Chloroacetyl chloride → 4-(1-Ethyl-1-cyclohexyloxycarbonyl)butyl methacrylate

HRID 225399

Reaktionsgleichung

C([C:3]1([OH:13])[CH:10]2[CH2:11]C3CC(CC1C3)[CH2:9]2)C.ClCC(Cl)=[O:17].[CH2:19]([C:21]1([OH:27])[CH2:26][CH2:25][CH2:24][CH2:23][CH2:22]1)[CH3:20].Cl[CH2:29][CH2:30][CH2:31][CH2:32][C:33](Cl)=[O:34]>>[C:3]([O:13][CH2:29][CH2:30][CH2:31][CH2:32][C:33]([O:27][C:21]1([CH2:19][CH3:20])[CH2:26][CH2:25][CH2:24][CH2:23][CH2:22]1)=[O:34])(=[O:17])[C:10]([CH3:11])=[CH2:9]

Komponenten

Edukt 4

HCID 6577Chloroacetyl chloride

HCID 160211-Ethylcyclohexanol

HCID 740895-Chlorovaleryl chloride

HCID 44019512-Ethyl-2-adamantanol

Produkt 1

HCID 689531604-(1-Ethyl-1-cyclohexyloxycarbonyl)butyl methacrylate

Versuchsvorschrift

Synthetic experiment was conducted in the same manner as in Monomer Synthesis Example 1 except that 2-ethyl-2-adamantanol and chloroacetyl chloride were changed to 1-ethyl-1-cyclohexanol and 5-chlorovaleryl chloride respectively, and the above described methacrylic derivative was obtained.

Aufarbeitung

customwas obtained

Quellen und Nachweise

ORD-Eintrag: ord-8361219c12a249c08926f238d10d0e29
Quelldatensatz: uspto-grants-2009_07
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07556908B2

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