Thionyl Chloride → HCID 10799500, Verbindung

HRID 2254403Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2254403
[CH2:1]([C:9]1[CH:10]=[C:11]([CH:14]=[CH:15][CH:16]=1)[CH2:12]O)[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.S(Cl)([Cl:19])=O>C(Cl)(Cl)Cl>[CH2:1]([C:9]1[CH:10]=[C:11]([CH:14]=[CH:15][CH:16]=1)[CH2:12][Cl:19])[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

Komponenten

4

Edukt 2

HCID 24386Thionyl ChlorideHCID 10488743Benzenemethanol, 3-(2-phenylethyl)-

Produkt 1

HCID 10799500HCID 10799500, VerbindungAusbeute 99 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 6212ChloroformLösungsmittel

Versuchsvorschrift

The resulting alcohol (140 mg) was dissolved in 1 ml of chloroform, and 0.3 ml of thionyl chloride was added. The mixture was reacted at room temperature for 30 minutes. The reaction mixture was evaporated under reduced pressure to give 150 mg (yield 99%) of 3-phenethylbenzyl chloride as a pale yellow oil.

Aufarbeitung

  1. customThe mixture was reacted at room temperature for 30 minutes
  2. customThe reaction mixture was evaporated under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-e0d091f11e3940e6979b2fad10b58995
Quelldatensatz
uspto-grants-1993_08
Patentnummer
US05234946

Notizen zur Reaktion

Wird geladen…