Sodium Hydroxide → HCID 19738055, Verbindung
Reaktionsgleichung
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH:9]([CH2:12][CH2:13][CH2:14][N:15]1[CH2:20][CH2:19][CH2:18][CH2:17][CH2:16]1)[C:10]#[N:11].Cl.Cl[CH2:23][N:24]1[CH:28]=[N:27][CH:26]=[N:25]1.[OH-].[Na+]>CS(C)=O>[C:10]([C:9]([C:3]1[CH:4]=[CH:5][C:6]([Cl:8])=[CH:7][C:2]=1[Cl:1])([CH2:12][CH2:13][CH2:14][N:15]1[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20]1)[CH2:23][N:24]1[CH:28]=[N:27][CH:26]=[N:25]1)#[N:11]Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
This compound (5.0 g.) was prepared using the procedure described in Example 9b except using 5.0 g. (0.016 mole) of 2-(2,4-dichlorophenyl)-5-(1-piperidinyl)valeronitrile, 2.7 g. (0.0176 mole) of 1-(chloromethyl)-1,2,4-triazole hydrochloride, 3.2 g. (0.040 mole) of aqueous 50% sodium hydroxide, and 50 ml. of DMSO and was isolated as an oil.