Ethanimidic acid, ethyl ester, hydrochloride (1:1) → HCID 178439387, Verbindung

HRID 2260040Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2260040
[NH2:1][C:2]1[CH:6]=[C:5]([CH2:7][CH2:8][CH3:9])[NH:4][N:3]=1.[ClH:10].[C:11](=[NH:16])(OCC)[CH3:12]>C(#N)C>[ClH:10].[CH2:7]([C:5]1[NH:4][N:3]=[C:2]([NH:1][C:11](=[NH:16])[CH3:12])[CH:6]=1)[CH2:8][CH3:9]

Komponenten

4

Edukt 2

HCID 2724290Ethanimidic acid, ethyl ester, hydrochloride (1:1)HCID 222656845-Propyl-1H-pyrazol-3-amine

Produkt 1

HCID 178439387HCID 178439387, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 6342AcetonitrileLösungsmittel

Versuchsvorschrift

A 11.5 g portion of 3-amino-5-propyl-1H-pyrazole was dissolved in 60 ml of acetonitrile, and 12.8 g of ethyl acetimidate hydrochloride was added to the above solution with cooling on an ice bath. The resulting mixture was stirred for 1 hour at the same temperature and then overnight at room temperature.

Aufarbeitung

  1. temperaturewith cooling on an ice bath
  2. customovernight
  3. customat room temperature

Quellen und Nachweise

ORD-Eintrag
ord-064c52bb5b48440fbb925e53e1ddedd9
Quelldatensatz
uspto-grants-1995_12
Patentnummer
US05475114

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