HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hexadecylamine → 3-(Hexadecylamino)propane-1,2-diol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hexadecylamine | HCID 8926 | — |
| Edukt | Glycidol | HCID 11164 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 3-(Hexadecylamino)propane-1,2-diol | HCID 111007 | — |
Reaktionsschritte
Hexadecylamine (5.00 g, 0.024 moles) was dissolved in absolute ethanol, and glycidol (3.07 g, 0.041 moles) was added dropwise. The reaction was refluxed under nitrogen for 4 hours then allowed to stir overnight. After 22 hours of refluxing, the reaction was stopped and a white solid formed during the cooling stage. The solid was recovered and recrystallized in hot hexane. (yield=2.02g)
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05476661 |
| Quelldatensatz | uspto-grants-1995_12 |
| ORD ID | ord-04890d8fb6154bda9211bfc8e6c4b477 |
| Quellennotiz | uspto-grants-1995_12 |