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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2260077Erstellt: 24. Oktober 2026

Hexadecylamine → 3-(Hexadecylamino)propane-1,2-diol

https://huagongshe.com/de/reaction/2260077

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHexadecylamineHCID 8926—
EduktGlycidolHCID 11164—
LösungsmittelEthanolHCID 702—
Produkt3-(Hexadecylamino)propane-1,2-diolHCID 111007—

Reaktionsschritte

Hexadecylamine (5.00 g, 0.024 moles) was dissolved in absolute ethanol, and glycidol (3.07 g, 0.041 moles) was added dropwise. The reaction was refluxed under nitrogen for 4 hours then allowed to stir overnight. After 22 hours of refluxing, the reaction was stopped and a white solid formed during the cooling stage. The solid was recovered and recrystallized in hot hexane. (yield=2.02g)

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05476661
Quelldatensatzuspto-grants-1995_12
ORD IDord-04890d8fb6154bda9211bfc8e6c4b477
Quellennotizuspto-grants-1995_12