Hexadecylamine → 3-(Hexadecylamino)propane-1,2-diol

HRID 2260077

Reaktionsgleichung

Reaktionsgleichung von HRID 2260077
[CH2:1]([NH2:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[CH2:18]1[O:20][CH:19]1[CH2:21][OH:22]>C(O)C>[OH:20][CH:19]([CH2:21][OH:22])[CH2:18][NH:17][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Komponenten

4

Edukt 2

HCID 8926HexadecylamineHCID 11164Glycidol

Produkt 1

HCID 1110073-(Hexadecylamino)propane-1,2-diol

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

Hexadecylamine (5.00 g, 0.024 moles) was dissolved in absolute ethanol, and glycidol (3.07 g, 0.041 moles) was added dropwise. The reaction was refluxed under nitrogen for 4 hours then allowed to stir overnight. After 22 hours of refluxing, the reaction was stopped and a white solid formed during the cooling stage. The solid was recovered and recrystallized in hot hexane. (yield=2.02g)

Aufarbeitung

  1. temperatureThe reaction was refluxed under nitrogen for 4 hours
  2. temperatureAfter 22 hours of refluxing
  3. customa white solid formed during the cooling stage
  4. customThe solid was recovered
  5. customrecrystallized in hot hexane

Quellen und Nachweise

ORD-Eintrag
ord-04890d8fb6154bda9211bfc8e6c4b477
Quelldatensatz
uspto-grants-1995_12
Patentnummer
US05476661

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