HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Glycidol → 3-(Octadecylamino)propane-1,2-diol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Glycidol | HCID 11164 | — |
| Edukt | Octadecylamine | HCID 15793 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 3-(Octadecylamino)propane-1,2-diol | HCID 120088 | — |
Reaktionsschritte
Octadecylamine (9.09 g, 0.034 mole) was dissolved in absolute ethanol. Glycidol (5.00 g, 0.068 mole) was added to the amine dropwise. The reaction solution was refluxed under nitrogen for 4 hours and then was stirred overnight at room temperature. A white solid was obtained (crude yield=10.8 g). The solid was recrystalized from hot hexane. (Yield=6.9 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05476671 |
| Quelldatensatz | uspto-grants-1995_12 |
| ORD ID | ord-2093b14d28454a6cadc580b9c2ddb3ce |
| Quellennotiz | uspto-grants-1995_12 |