Potassium Hydroxide → HCID 15825476, Verbindung

HRID 2260094

Reaktionsgleichung

Reaktionsgleichung von HRID 2260094
[OH:1][CH:2]([CH2:21][OH:22])[CH2:3][NH:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20].[OH-].[K+].[OH:25][CH:26]([CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH3:44])[C:27]([O:29]C)=O>>[OH:1][CH:2]([CH2:21][OH:22])[CH2:3][N:4]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])[C:27](=[O:29])[CH:26]([OH:25])[CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH3:44]

Komponenten

4

Edukt 3

HCID 14797Potassium HydroxideHCID 1110073-(Hexadecylamino)propane-1,2-diolHCID 543716Methyl 2-hydroxyhexadecanoate

Produkt 1

HCID 15825476HCID 15825476, Verbindung

Versuchsvorschrift

N-(2,3-dihydroxypropyl)-N-hexadecylamine (1.0 g, 0.0032 mole) and potassium hydroxide (0.01 g, 0.18 mmole) were heated to 85° C. under vacuum and methyl 2-hydroxyhexadecanoate (0.907 g, 0.0032 mole) was heated and added dropwise to the reaction. The reaction was heated under vacuum for 6 hours. A waxy off-white solid was obtained (crude yield=1.79 g). The waxy solid was recrystalized from hot hexane (yield=0.94 g).

Aufarbeitung

  1. temperaturewas heated
  2. additionadded dropwise to the reaction
  3. temperatureThe reaction was heated under vacuum for 6 hours
  4. customA waxy off-white solid was obtained (crude yield=1.79 g)
  5. customThe waxy solid was recrystalized from hot hexane (yield=0.94 g)

Quellen und Nachweise

ORD-Eintrag
ord-b95a455865cc49fc8505d782444943a7
Quelldatensatz
uspto-grants-1995_12
Patentnummer
US05476671

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