HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Methoxy-N-(4-methoxyphenyl)benzylamine → N-[(4-methoxyphenyl)methyl]-N-(4-methoxyphenyl)-7-methoxy-1,2,3,4-tetrahydronaphthalene-1-carboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Methoxy-N-(4-methoxyphenyl)benzylamine | HCID 4131497 | — |
| Edukt | 7-Methoxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid | HCID 13277484 | — |
| Produkt | N-[(4-methoxyphenyl)methyl]-N-(4-methoxyphenyl)-7-methoxy-1,2,3,4-tetrahydronaphthalene-1-carboxamide | HCID 59597406 | 46,1% |
Reaktionsschritte
By the reaction and treatment in the same manner as in Example 1 using 7-methoxy-1,2,3,4-tetrahydronaphthalene-1-carboxylic acid (1.5 g) and [(4-methoxyphenyl)methyl](4-methoxyphenyl)amine (0.88 g) as starting materials, N-[(4-methoxyphenyl)methyl]-N-(4-methoxyphenyl)-7-methoxy-1,2,3,4-tetrahydronaphthalene-1-carboxamide (0.72 g) was obtained. melting point: 89-90° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07855297B2 |
| Quelldatensatz | uspto-grants-2010_12 |
| ORD ID | ord-bd78e0e7d19b4fd081a1a52c86c77f33 |
| Quellennotiz | uspto-grants-2010_12 |