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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 226981Erstellt: 25. Oktober 2026

Diphenyl Ether → 3-(3,4-Dimethyl-benzoyl)-6-methyl-1H-[1,5]naphthyridin-4-one

https://huagongshe.com/reaction/226981

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktDiphenyl EtherHCID 7583—
Edukt5-Amino-2-methylpyridineHCID 243313—
Edukt2-(3,4-Dimethyl-benzoyl)-3-methoxy-acrylic acid methyl esterHCID 66879272—
Produkt3-(3,4-Dimethyl-benzoyl)-6-methyl-1H-[1,5]naphthyridin-4-oneHCID 5775478322%

Reaktionsschritte

Experimental conditions analogous to those described for step 1 of Example 1 were used with 0.50 g (2.01 mmol) 2-(3,4-Dimethyl-benzoyl)-3-methoxy-acrylic acid methyl ester, 0.22 g (2.01 mmol) of 6-Methyl-pyridin-3-ylamine, and 15 mL of diphenyl ether to yield 129 mg of 3-(3,4-Dimethyl-benzoyl)-6-methyl-1H-[1,5]naphthyridin-4-one as a brown solid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07557213B2
Quelldatensatzuspto-grants-2009_07
ORD IDord-f916954bb573487591ccb30dc54b5a24
Quellennotizuspto-grants-2009_07