(5-Methylthiophen-2-yl)boronic acid → N-[5-(5-methyl-2-thienyl)thiophene-2-sulfonyl]pyrrole

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	(5-Methylthiophen-2-yl)boronic acid	HCID 2734374	—
Edukt	N-(5-bromothiophenesulfonyl)pyrrole	HCID 23445587	—
Produkt	N-[5-(5-methyl-2-thienyl)thiophene-2-sulfonyl]pyrrole	HCID 22998476	72%

Reaktionsschritte

N-[5-(5-methyl-2-thienyl)thiophene-2-sulfonyl]pyrrole was prepared in the same manner as described in Example 32C from 2-methylthiophene-5-boronic acid and N-(5-bromothiophene-2-sulfonyl) pyrrole. Purification by column chromatography using 2% ether/hexanes gave the pure sulfonamide in 72% yield as a white solid.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US06331637B1
Quelldatensatz	uspto-grants-2001_12
ORD ID	ord-b28905de5e0746b3928326fe6ffcf578
Quellennotiz	uspto-grants-2001_12