Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 227088Erstellt: 25. Oktober 2026

Lithium Hydroxide → 1-(4-Methoxybenzyl)-4-oxo-1,4-dihydroquinoline-3-carboxylic acid

https://huagongshe.com/reaction/227088

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktLithium HydroxideHCID 3939—
EduktEthyl 1-(4-methoxybenzyl)-4-oxo-1,4-dihydroquinoline-3-carboxylateHCID 53396422—
LösungsmittelMethanol--water (1/1)HCID 22242641—
Produkt1-(4-Methoxybenzyl)-4-oxo-1,4-dihydroquinoline-3-carboxylic acidHCID 1476756—

Reaktionsschritte

Experimental conditions analogous to those described for Step 4 of Example 60, from 3.10 g (8.80 mmol) of 1-(4-methoxy-benzyl)-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid ethyl ester, 40 mL of 1:1 methanol-water mixture and 0.44 g (18.3 mmol) of lithium hydroxide with a work-up consisting only of thorough evaporation of solvents.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07557213B2
Quelldatensatzuspto-grants-2009_07
ORD IDord-3555beaeacb04c9e94925aaf9e04f70f
Quellennotizuspto-grants-2009_07