[CH3:1][C:2]1([CH3:22])[CH:14]=[C:13]2[C:5](=[C:6]3[C:11](=[CH:12]2)[CH:10]=[CH:9][C:8]2[CH:15]=[CH:16][C:17](B(O)O)=[CH:18][C:7]3=2)[CH:4]=[CH:3]1.Br[C:24]1[CH:25]=[C:26]([C:31]2[N:36]=[C:35]([C:37]3[CH:42]=[CH:41][CH:40]=[CH:39][CH:38]=3)[N:34]=[C:33]([C:43]3[CH:48]=[CH:47][CH:46]=[CH:45][CH:44]=3)[N:32]=2)[CH:27]=[C:28](Br)[CH:29]=1.C([O-])([O-])=O.[K+].[K+].[N:55]1[CH:60]=[CH:59][CH:58]=[CH:57][C:56]=1[C:61]1[CH:66]=[CH:65][C:64](B(O)O)=[CH:63][CH:62]=1>C1C=CC([P]([Pd]([P](C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)([P](C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)[P](C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)=CC=1.C(O)C.C1(C)C=CC=CC=1>[CH3:1][C:2]1([CH3:22])[CH:14]=[C:13]2[C:5](=[C:6]3[C:11](=[CH:12]2)[CH:10]=[CH:9][C:8]2[CH:15]=[CH:16][C:17]([C:24]4[CH:25]=[C:26]([C:31]5[N:36]=[C:35]([C:37]6[CH:42]=[CH:41][CH:40]=[CH:39][CH:38]=6)[N:34]=[C:33]([C:43]6[CH:48]=[CH:47][CH:46]=[CH:45][CH:44]=6)[N:32]=5)[CH:27]=[C:28]([C:64]5[CH:63]=[CH:62][C:61]([C:56]6[CH:57]=[CH:58][CH:59]=[CH:60][N:55]=6)=[CH:66][CH:65]=5)[CH:29]=4)=[CH:18][C:7]3=2)[CH:4]=[CH:3]1In a stream of argon, 185 mg (0.644 mmol) of 9,9-dimethyl-2-benzo[c]fluoreneboronic acid, 300 mg (0.644 mmol) of 2-(3,5-dibromophenyl)-4,6-diphenyl-1,3,5-triazine and 7.44 mg (0.00644 mmol) of tetrakis(triphenylphosphine)palladium were suspended in a mixed solvent composed of 24 mL of toluene and 3 mL of ethanol, and the resultant suspension was heated to 50° C. To the suspension, 1.93 ml (1.93 mmol) of an aqueous 1M K2CO3 solution was gradually added dropwise, and the mixture was stirred for 3 hours. The resultant reaction mixture was heated to 80° C. and further stirred for 3 hours. The reaction mixture was cooled to room temperature, and then, 256 mg (1.29 mmol) of 4-(2-pyridyl)phenylboronic acid and 2.90 mL (2.90 mmol) of an aqueous 1M K2CO3 solution were added to the reaction mixture. The resultant mixture was heated to 80° C., and maintained at that temperature for 24 hours while being stirred. The obtained reaction mixture was cooled to room temperature, and then distilled under a reduced pressure to remove all volatile materials. Methanol was added to the concentrate, and the thus-deposited solid was collected by filtration. The obtained crude product was purified by silica gel chromatography using a hexane/chloroform (1:2) mixed solvent as an eluent to give 172 mg of the target 2-[5-(9,9-dimethylbenzo[c]fluoren-2-yl)-4′-(2-pyridyl)biphenyl-3-yl]-4,6-diphenyl-1,3,5-triazine as a white solid (yield: 38.0%).
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