HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triethylamine → 1,3-Dioxolan-4-ylmethyl methanesulfonate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | 1,3-Dioxolane-4-methanol | HCID 21618 | — |
| Edukt | Methanesulfonyl chloride | HCID 31297 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | 1,3-Dioxolan-4-ylmethyl methanesulfonate | HCID 87145518 | — |
Reaktionsschritte
The glycerol formal (Aldrich, 0.26 g, 2.5 mmol), triethylamine (1.1 mL, 8.3 mmol), and methanesulfonyl chloride (0.30 mL, 3.7 mmol) in 20 mL THF were processed as described in Example 1C to give the title compound that was used directly in the next reaction.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07560481B2 |
| Quelldatensatz | uspto-grants-2009_07 |
| ORD ID | ord-8fa5e47351eb4d72a032b15200704450 |
| Quellennotiz | uspto-grants-2009_07 |