2-Fluoro-5-hydrazinylbenzonitrile → 2-Fluoro-8-methoxy-6,6-dimethyl-6,11-dihydro-5H-benzo[b]carbazole-3-carbonitrile
Reaktionsgleichung
[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH2:7][CH2:8][C:9](=O)[C:10]2([CH3:14])[CH3:13])=[CH:5][CH:4]=1.[C:16]([C:18]1[CH:19]=[C:20]([NH:25]N)[CH:21]=[CH:22][C:23]=1[F:24])#[N:17]>>[F:24][C:23]1[CH:22]=[C:21]2[C:20](=[CH:19][C:18]=1[C:16]#[N:17])[NH:25][C:9]1[C:10]([CH3:14])([CH3:13])[C:11]3[CH:12]=[C:3]([O:2][CH3:1])[CH:4]=[CH:5][C:6]=3[CH2:7][C:8]2=1Komponenten
3
Versuchsvorschrift
Under the same conditions as the method for synthesizing Compound A3-1, the title compound was prepared from Compound A2 and 3-cyano-4-fluorophenylhydrazine.
Aufarbeitung
- customUnder the same conditions as the method for synthesizing Compound A3-1