HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Amino-4,6-dimethyl pyrimidine → (5,7-Dimethyl-2-pyridin-2-yl-imidazo[1,2-a]-pyrimidin-3-yl)-(6-isocyanohexyl)amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Amino-4,6-dimethyl pyrimidine | HCID 13021 | — |
| Edukt | 2-Pyridinecarboxaldehyde | HCID 14273 | — |
| Edukt | 1,6-Diisocyanohexane | HCID 3391105 | — |
| Lösungsmittel | Perchloric Acid | HCID 24247 | — |
| Produkt | (5,7-Dimethyl-2-pyridin-2-yl-imidazo[1,2-a]-pyrimidin-3-yl)-(6-isocyanohexyl)amine | HCID 15521056 | — |
Reaktionsschritte
Compound (2) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-4,6-dimethylpyrimidine solution (0.1 M, DCM), 0.575 ml of 1,6-diisocyanhexane solution (0.2 M, DCM), 0.500 ml of pyridine-2-carbaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06849642B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-09d402d3ada54c4694616c3ca8d33b2a |
| Quellennotiz | uspto-grants-2005_02 |