HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Perchloric Acid → (8-Benzyloxy-2-cyclohexylimidazo[1,2-a]pyridin-3-ylamino)-acetic acid methyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Perchloric Acid | HCID 24247 | — |
| Edukt | 2-Amino-3-benzyloxypyridine | HCID 90334 | — |
| Edukt | Methyl isocyanoacetate | HCID 547815 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | (8-Benzyloxy-2-cyclohexylimidazo[1,2-a]pyridin-3-ylamino)-acetic acid methyl ester | HCID 69732054 | — |
Reaktionsschritte
Compound (30) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-3-benzyloxypyridine solution (0.1 M, DCM), 0.575 ml of methyl isocyanoacetate solution (0.2 M, DCM), 0.500 ml of cyclohexylcarbaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06849642B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-f5bdd3d63b7542b3a523339961db6ca0 |
| Quellennotiz | uspto-grants-2005_02 |