P-Phenylenediamine → N,N'-(1,4-phenylene)bis(2-(4-cyanophenyl)-1H-benzo[d]imidazole-5-carboxamide)
Reaktionsgleichung
[C:1]([C:3]1[CH:8]=[CH:7][C:6]([C:9]2[NH:10][C:11]3[CH:17]=[C:16]([C:18](O)=[O:19])[CH:15]=[CH:14][C:12]=3[N:13]=2)=[CH:5][CH:4]=1)#[N:2].[C:21]1([NH2:28])[CH:26]=[CH:25][C:24]([NH2:27])=[CH:23][CH:22]=1>>[C:21]1([NH:28][C:18]([C:16]2[CH:15]=[CH:14][C:12]3[NH:13][C:9]([C:6]4[CH:5]=[CH:4][C:3]([C:1]#[N:2])=[CH:8][CH:7]=4)=[N:10][C:11]=3[CH:17]=2)=[O:19])[CH:26]=[CH:25][C:24]([NH:27][C:18]([C:16]2[CH:15]=[CH:14][C:12]3[NH:13][C:9]([C:6]4[CH:5]=[CH:4][C:3]([C:1]#[N:2])=[CH:8][CH:7]=4)=[N:10][C:11]=3[CH:17]=2)=[O:19])=[CH:23][CH:22]=1Komponenten
3
Versuchsvorschrift
Compound 281 was prepared according to the procedure similar to that described in Scheme V from 2-(4-cyanophenyl)benzimidazole-5-carboxylic acid and 1,4-phenylenediamine. [M+H]+ calcd for C36H22N8O2: 599.19; found: 598.97.
Quellen und Nachweise
- ORD-Eintrag
- ord-c563411662fe47d190afa18f112e7a8e
- Quelldatensatz
- uspto-grants-2015_09