1-Chlorododecane → 3-Dimethylaminopropyl Laurate

HRID 2285676

Reaktionsgleichung

Reaktionsgleichung von HRID 2285676
[CH3:1][N:2]([CH3:7])[CH2:3][CH2:4][CH2:5][OH:6].[CH2:8](Cl)[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19].[OH-:21].[Na+]>C(Cl)(Cl)Cl>[C:8]([O:6][CH2:5][CH2:4][CH2:3][N:2]([CH3:7])[CH3:1])(=[O:21])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]

Komponenten

5

Edukt 3

HCID 81921-ChlorododecaneHCID 14798Sodium HydroxideHCID 766463-(Dimethylamino)-1-propanol

Produkt 1

HCID 36130803-Dimethylaminopropyl Laurate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 6212ChloroformLösungsmittel

Versuchsvorschrift

In accordance with the procedure of Example 10, 72.2 g of 3-dimethylamino-1-propanol and 153.1 g of lauryl chloride are reacted in altogether 250 ml of CHCl3. The reaction mixture is neutralised with 147 ml of 20% NaOH. Yield: 157.2 g (82.1%) of product with a boiling point of 110° C./0.01 torr.

Quellen und Nachweise

ORD-Eintrag
ord-ad094bf6a17648be8caf3218bdd098ce
Quelldatensatz
uspto-grants-1982_04
Patentnummer
US04324739

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