HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(4,5-Dimethylfuran-2-yl)-(4,5-dimethylthiazol-2-yl)methanol → (4,5-Dimethylfuran-2-yl)(4,5-dimethylthiazol-2-yl)-methanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (4,5-Dimethylfuran-2-yl)-(4,5-dimethylthiazol-2-yl)methanol | HCID 23078354 | — |
| Katalysator | HCID 178418406 | HCID 178418406 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | (4,5-Dimethylfuran-2-yl)(4,5-dimethylthiazol-2-yl)-methanone | HCID 23078247 | 97,1% |
Reaktionsschritte
(4,5-Dimethylfuran-2-yl)-(4,5-dimethylthiazol-2-yl)methanol (945 mg) was dissolved in chloroform (20 ml) to prepare a solution. Manganese dioxide (3.5 g) was added to the solution, and the mixture was stirred at room temperature overnight. The reaction solution was filtered through Celite, and the solvent was removed from the filtrate by distillation under the reduced pressure to give (4,5-dimethylfuran-2-yl)(4,5-dimethylthiazol-2-yl)-methanone (910 mg, yield 97%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07560558B2 |
| Quelldatensatz | uspto-grants-2009_07 |
| ORD ID | ord-ff9c0126c13c495080a3055c9946dee9 |
| Quellennotiz | uspto-grants-2009_07 |