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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 228818Erstellt: 25. Oktober 2026

(4,5-Dimethylfuran-2-yl)-(6-methyl-pyridin-2-yl)-methanol → (4,5-Dimethylfuran-2-yl)-(6-methyl-pyridin-2-yl)methanone

https://huagongshe.com/reaction/228818

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt(4,5-Dimethylfuran-2-yl)-(6-methyl-pyridin-2-yl)-methanolHCID 23078353—
KatalysatorHCID 178418406HCID 178418406—
LösungsmittelChloroformHCID 6212—
Produkt(4,5-Dimethylfuran-2-yl)-(6-methyl-pyridin-2-yl)methanoneHCID 2307839058,8%

Reaktionsschritte

(4,5-Dimethylfuran-2-yl)-(6-methyl-pyridin-2-yl)-methanol (1.4 g) was dissolved in chloroform (30 ml) to prepare a solution. Manganese dioxide (5.7 g) was added to the solution, and the mixture was stirred at room temperature overnight. Further, manganese dioxide (1.8 g) was then added thereto, and the mixture was stirred overnight. The reaction solution was filtered through Celite. The solvent was removed from the filtrate by distillation under the reduced pressure to give (4,5-dimethylfuran-2-yl)-(6-methyl-pyridin-2-yl)-methanone (815 mg, yield 58%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07560558B2
Quelldatensatzuspto-grants-2009_07
ORD IDord-6ab18d8b261b491b95b95d5380da68f3
Quellennotizuspto-grants-2009_07