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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 229049Erstellt: 23. Oktober 2026

(4,5-Dimethylfuran-2-yl)-(3-methylpyridin-2-yl)-methanol → (4,5-Dimethylfuran-2-yl)-(3-methylpyridin-2-yl)-methanone

https://huagongshe.com/de/reaction/229049

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt(4,5-Dimethylfuran-2-yl)-(3-methylpyridin-2-yl)-methanolHCID 23078465—
KatalysatorHCID 178418406HCID 178418406—
LösungsmittelChloroformHCID 6212—
Produkt(4,5-Dimethylfuran-2-yl)-(3-methylpyridin-2-yl)-methanoneHCID 2307852981,1%

Reaktionsschritte

(4,5-Dimethylfuran-2-yl)-(3-methylpyridin-2-yl)-methanol (1.17 g) was dissolved in chloroform (30 ml) to prepare a solution. Manganese dioxide (4.69 g) was added to the solution, and the mixture was stirred at room temperature overnight. The reaction solution was filtered through Celite, and the solvent was removed from the filtrate by distillation under the reduced pressure to give (4,5-dimethylfuran-2-yl)-(3-methylpyridin-2-yl)-methanone (940 mg, yield 81%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07560558B2
Quelldatensatzuspto-grants-2009_07
ORD IDord-d541dd2f8c2b40be824318bccb382ad9
Quellennotizuspto-grants-2009_07