HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 1,3,5-Tris-(p-(oct-1-yloxycarbonyl)-anilino)-s-triazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Cyanuric chloride | HCID 7954 | — |
| Edukt | Octyl p-aminobenzoate | HCID 26629 | — |
| Lösungsmittel | O-Xylene | HCID 7237 | — |
| Produkt | 1,3,5-Tris-(p-(oct-1-yloxycarbonyl)-anilino)-s-triazine | HCID 20152733 | — |
Reaktionsbedingungen
| Temperatur | 90 °C |
|---|
Reaktionsschritte
75 g of octyl p-aminobenzoate and 18.5 g of cyanuric chloride in 1,000 ml of xylene were heated at 140° C. for 8 hours. After the evolution of hydrogen chloride was complete, the reaction solution was cooled to 90° C., washed twice with saturated sodium bicarbonate solution and once with water and then cooled to room temperature. The white crystals precipitated were filtered off under suction.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04617390 |
| Quelldatensatz | uspto-grants-1986_10 |
| ORD ID | ord-406a8ee66c394100acc9d9181a37e888 |
| Quellennotiz | uspto-grants-1986_10 |